N2-(4-Methoxyphenyl)pyrimidine-2,5-diamine synthesis

1synthesis methods

Product Name:N2-(4-Methoxyphenyl)pyrimidine-2,5-diamine
CAS Number:26806-77-9
Molecular formula:C11H12N4O
Molecular Weight:216.24

104-92-7 Synthesis

104-92-7
426 suppliers
$10.00/10g

N2-(4-Methoxyphenyl)pyrimidine-2,5-diamine

26806-77-9
6 suppliers
$469.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 18 h / Heating / reflux
2: hydrogen / palladium 10% on activated carbon / methanol / 4 h

References:

WO2008/8234,2008,A1