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ChemicalBook CAS DataBase List N2,N2-diMethylpyridine-2,6-diaMine

N2,N2-diMethylpyridine-2,6-diaMine synthesis

2synthesis methods
-

Yield:63763-86-0 73%

Reaction Conditions:

with dimethyl amine in ethanol;

Steps:

47.A A.

A. 2-Amino-6-dimethylaminopyridine The title compound is obtained from the reaction of 2-amino-6-bromopyridine and dimethylamine in ethanol at 180° in a pressure vessel fro 36 hours. The product is distilled and then recrystallized from hexane, m.p. 58°-60°. The yield is 73%.

References:

US4203988,1980,A