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333366-23-7

N3-Asp(tBu)-OH (dicyclohexylammonium) salt synthesis

1synthesis methods
3057-74-7 Synthesis
L-Aspartic acid 4-tert-butyl ester

3057-74-7
242 suppliers
$5.00/1g

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Yield:333366-23-7 88%

Reaction Conditions:

with imidazole-1-sulfonyl azide hydrochloride;copper(ll) sulfate pentahydrate;potassium carbonate in methanol at 20; for 18 h;

References:

Valverde, Ibai E.;Lecaille, Fabien;Lalmanach, Gilles;Aucagne, Vincent;Delmas, Agnes F. [Angewandte Chemie - International Edition,2012,vol. 51,# 3,p. 718 - 722] Location in patent:supporting information; experimental part