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ChemicalBook CAS DataBase List N3-L-Lys(Fmoc)-OH

N3-L-Lys(Fmoc)-OH synthesis

3synthesis methods
L-Lysine, N6-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2,2-trifluoroacetate (1:1)

84624-29-3
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N3-L-Lys(Fmoc)-OH

473430-12-5
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Yield:473430-12-5 92%

Reaction Conditions:

with triflic azide;potassium carbonate;copper(II) sulfate in methanol;dichloromethane;water; for 1 h;

References:

Saludes, Jonel P.;Ames, James B.;Gervay-Hague, Jacquelyn [Journal of the American Chemical Society,2009,vol. 131,p. 5495 - 5505] Location in patent:supporting information; scheme or table