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613-79-6

Naphthalene, 2,2'-methylenebis- synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 2 h / -78 - 20 °C
2.1: trifluoroacetic acid; sodium tetrahydroborate / 70 min / 20 °C

References:

Hou, Liuzhen;Zhou, Yuqiao;Yu, Han;Zhan, Tangyu;Cao, Weidi;Feng, Xiaoming [Journal of the American Chemical Society,2022,vol. 144,# 48,p. 22140 - 22149]