NICOTINIC ACID-CARBOXY-14C synthesis
1synthesis methods
- Product Name:NICOTINIC ACID-CARBOXY-14C
- CAS Number:2906-42-5
- Molecular formula:C6H5NO2
- Molecular Weight:125.13
![CARBON DIOXIDE, [14C]](/CAS/GIF/51-90-1.gif)
Yield:2906-42-5 58%
Reaction Conditions:
Stage #1: 3-Bromopyridinewith n-butyllithium in diethyl ether at -70; for 1.16667 h;
Stage #2: [14C]carbon dioxide at -70;Cooling with liquid nitrogen;
References:
Elmore, Charles S.;Landvatter, Scott;Dorff, Peter N.;Powell, Mark E.;Killick, David;Blake, Timothy;Hall, James;Heys, J. Richard;Harding, John;Urbanek, Rebecca;Ernst, Glen [Journal of labelled compounds and radiopharmaceuticals,2014,vol. 57,# 5,p. 342 - 349]