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ChemicalBook CAS DataBase List NISTC3228044

NISTC3228044 synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: N-chlorosuccinimide (NCS) / CH2Cl2 / 0.5 h / -25 °C
2: triethylamine / CH2Cl2 / 4 h / Ambient temperature
3: W2 Raney nickel / ethanol / 24 h / Heating

References:

James, Roger;Glen, John B. [Journal of Medicinal Chemistry,1980,vol. 23,# 12,p. 1350 - 1357]