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ChemicalBook CAS DataBase List Nsc41608

Nsc41608 synthesis

6synthesis methods
2676-33-7 Synthesis
(S)-Ethyl 2-hydroxypropionate

2676-33-7
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ethyl (±)-2-bromopropionate

41978-69-2
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Yield:6937-25-3 84%

Reaction Conditions:

with sodium hydride in tetrahydrofuran;mineral oil at 0 - 20; for 2 h;Reflux;

References:

Iqbal, Mudassir;Huskens, Jurriaan;Verboom, Willem;Sypula, Michal;Modolo, Giuseppe [Supramolecular Chemistry,2010,vol. 22,# 11-12,p. 827 - 837] Location in patent:experimental part