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NSC57674 synthesis

1synthesis methods
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Yield:7155-00-2 90%

Reaction Conditions:

with [bis(acetoxy)iodo]benzene;ammonium carbamate in methanol at 25; for 24 h;Inert atmosphere;chemoselective reaction;

References:

Tota, Arianna;St John-Campbell, Sahra;Briggs, Edward L.;Estévez, Gala Ogalla;Afonso, Michelle;Degennaro, Leonardo;Luisi, Renzo;Bull, James A. [Organic Letters,2018,vol. 20,# 9,p. 2599 - 2602] Location in patent:supporting information