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O-ethyl thioformate synthesis

2synthesis methods
-

Yield:29392-46-9 83%

Reaction Conditions:

with sulfuric acid;hydrogen sulfide under 1275.13 - 1575.16 Torr; for 3 h;Inert atmosphere;

References:

Borths, Christopher J.;Chan, Johann;Burke, Brenda J.;Larsen, Robert D. [Synlett,2009,# 19,p. 3139 - 3142] Location in patent:experimental part