(o-Nitrophenyl)-p-benzoquinone synthesis
1synthesis methods
- Product Name:(o-Nitrophenyl)-p-benzoquinone
- CAS Number:105946-79-0
- Molecular formula:C12H7NO4
- Molecular Weight:229.19
Yield: 84%
Reaction Conditions:
Stage #1:2-nitro-aniline with methanesulfonic acid;2,2-dimethylpropyl nitrite in water at 25; for 0.166667 h;Green chemistry;
Stage #2:p-benzoquinone in water at 20; for 12 h;Irradiation;Green chemistry;
References:
Wang, Liang;Shen, Jun;Yang, Sen;Liu, Wenjie;Chen, Qun;He, Mingyang [Green Chemistry,2018,vol. 20,# 6,p. 1290 - 1296] Location in patent:supporting information