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ChemicalBook CAS DataBase List O-(TERT-BUTYLDIMETHYLSILYL)BENZANILIDE

O-(TERT-BUTYLDIMETHYLSILYL)BENZANILIDE synthesis

1synthesis methods
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Yield:404392-70-7 83%

Reaction Conditions:

Stage #1: N-phenyl benzoyl amidewith sodium hydride in acetonitrile at 20 - 25; for 1 h;
Stage #2: tert-butyldimethylsilyl chloride in acetonitrile at 20 - 25;Further stages.;

References:

Misaki;Kurihara;Tanabe [Chemical Communications,2001,# 23,p. 2478 - 2479]