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ChemicalBook CAS DataBase List Oxaflozane
26629-87-8

Oxaflozane synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 92.9 percent / Br2 / CHCl3 / 1.5 h / Ambient temperature
2: 65.1 percent / toluene / 24 h / Ambient temperature
3: 79.1 percent / p-toluenesulfonic acid monohydrate / benzene / 2 h / Heating
4: 66 percent / H2 / PtO2 / acetic acid / 18 h

References:

Weintraub, Philip M.;Meyer, Donald R.;Aiman, Charles E. [Journal of Organic Chemistry,1980,vol. 45,# 24,p. 4989 - 4990]