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Oxiranemethanol, 3-ethynyl-alpha,2-dimethyl- (9CI) synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: diethyl ether
2: aq. H2SO4 / diethyl ether
3: m-chloroperbenzoic acid / CH2Cl2 / 2.25 h / 0 - 20 °C

References:

Piotti, Marcelo E.;Alper, Howard [Journal of Organic Chemistry,1997,vol. 62,# 24,p. 8484 - 8489]