ChemicalBook CAS DataBase List p-Anisidine, 2,6-dinitro-,

p-Anisidine, 2,6-dinitro-, synthesis

11synthesis methods

Product Name:p-Anisidine, 2,6-dinitro-,
CAS Number:5350-56-1
Molecular formula:C7H7N3O5
Molecular Weight:213.15

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Yield:5350-56-1 53%

Reaction Conditions:

with nitric acid in water at 20;

Steps:

59 INTERMEDIATE 59 4-methoxy-2,6-dinitro-phenylamine

To a stirred solution of HNO3 (65 mL) was added 4-methoxy-2-nitro-phenylamine (15 g, 89.3 mmol). The reaction mixture was stirred at room temperature overnight. The dark red precipitate was filtered and washed with H2O (400 mL) affording 10.01 g (53%) of the title compound

References:

EP1147083,2004,B1 Location in patent:Page 48

5327-44-6 Synthesis