P-AZIDOPHENYL SULFONE synthesis
- Product Name:P-AZIDOPHENYL SULFONE
- CAS Number:7300-27-8
- Molecular formula:C12H8N6O2S
- Molecular Weight:300.3
80-08-0
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7300-27-8
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$82.00/1g
Yield:7300-27-8 96%
Reaction Conditions:
Stage #1: 4,4'-diaminodiphenyl sulphonewith 1-methyl-2-oxopyrrolidinium hydrogen sulfate in water monomer at 20; for 0.0166667 h;Grinding;
Stage #2: with NaNO2 in water monomer at 20;Grinding;
Stage #3: with Caswell No. 744A in water monomer at 20;Grinding;
References:
Hajipour, Abdol Reza;Mohammadsaleh, Fatemeh [Organic Preparations and Procedures International,2011,vol. 43,# 5,p. 451 - 455] Location in patent:experimental part