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ChemicalBook CAS DataBase List P-fluorophenyltriMethoxysilane

P-fluorophenyltriMethoxysilane synthesis

1synthesis methods
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Yield: 64%

Reaction Conditions:

Stage #1:1-Bromo-4-fluorobenzene with hydrogenchloride;iodine;magnesium in methanol;diethyl etherReflux;
Stage #2:tetramethylorthosilicate in methanol;diethyl ether at -5 - 23;

References:

Visco, Michael D.;Wieting, Joshua M.;Mattson, Anita E. [Organic Letters,2016,vol. 18,# 12,p. 2883 - 2885] Location in patent:supporting information