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Pentanenitrile, 5-aMino- synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / NaN3 / acetone; H2O / 20 °C
2: 1,1-diazenediyldicyclohexanecarbonitrile; tert-dodecanethiol / toluene / 4 h / 110 °C
3: H2O / 20 °C

References:

Benati, Luisa;Bencivenni, Giorgio;Leardini, Rino;Minozzi, Matteo;Nanni, Daniele;Scialpi, Rosanna;Spagnolo, Piero;Zanardi, Giuseppe [Journal of Organic Chemistry,2006,vol. 71,# 15,p. 5822 - 5825]