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ChemicalBook CAS DataBase List Phenol, 3-aMino-2-broMo-

Phenol, 3-aMino-2-broMo- synthesis

5synthesis methods
56619-93-3 Synthesis
N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE

56619-93-3
86 suppliers
$22.00/1g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) n-BuLi, 2.) bromine / 1.) THF, hexane, 0 deg C, 2.5 h, 2.) THF, hexane, -78 deg C, 1 h
2: 1.) AlCl3 / 1.) CS2, reflux, 3 h, 2.) 70 deg C, 2 d
3: 61 percent / ethanolic HCl / 12 h / 80 °C

References:

Kozikowski, Alan P.;Ma, Dawei;Du, Linh;Lewin, Nancy E.;Blumberg, Peter M. [Journal of the American Chemical Society,1995,vol. 117,# 25,p. 6666 - 6672]