![](/CAS/GIF/1885-14-9.gif)
Phenyl chloroformate synthesis
- Product Name:Phenyl chloroformate
- CAS Number:1885-14-9
- Molecular formula:C7H5ClO2
- Molecular Weight:156.57
![Phenol](/CAS/20180808/GIF/108-95-2.gif)
108-95-2
719 suppliers
$14.00/25g
![Phenyl chloroformate](/CAS/GIF/1885-14-9.gif)
1885-14-9
332 suppliers
$10.00/1g
Yield:1885-14-9 91.5%
Reaction Conditions:
with CoCl2 in triphenylphosphine;
Steps:
4.b Example 4
(b) A further 500 g of phenol are added to the residue, which weighs 100 g, without feeding in fresh triphenylphosphine. The reaction is carried out, as described under 4(a), with 560 g of COCl2. After a phosgenation time of 8 hours, 764 g of distilled 99.7% pure chloroformic acid phenyl ester are obtained (91.5% of the theoretical yield).
References:
US4366102,1982,A
![Triphosgene](/CAS/GIF/32315-10-9.gif)
32315-10-9
410 suppliers
$10.00/1g
![Phenol](/CAS/20180808/GIF/108-95-2.gif)
108-95-2
719 suppliers
$14.00/25g
![Phenyl chloroformate](/CAS/GIF/1885-14-9.gif)
1885-14-9
332 suppliers
$10.00/1g
![Carbonic acid, monophenyl ester](/CAS/20200515/GIF/13932-55-3.gif)
13932-55-3
2 suppliers
inquiry
![Phenyl chloroformate](/CAS/GIF/1885-14-9.gif)
1885-14-9
332 suppliers
$10.00/1g
![2-Thiophenecarboxylic acid, 5-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-, ethyl ester](/CAS/20200611/GIF/851443-09-9.gif)
851443-09-9
0 suppliers
inquiry
![Phenyl chloroformate](/CAS/GIF/1885-14-9.gif)
1885-14-9
332 suppliers
$10.00/1g