phenyl(tribromomethyl)mercury synthesis
1synthesis methods
- Product Name:phenyl(tribromomethyl)mercury
- CAS Number:3294-60-8
- Molecular formula:C7H5Br3Hg
- Molecular Weight:529.4166
Yield:3294-60-8 95%
Reaction Conditions:
with potassium hydroxide in Bromoform;water;an aq. KOH soln. was added to react. mixt. at 25 °C, stirred 2 h; washed (H2O), extd. (Et2O), org. layer was dried (anhyd. MgSO4), filtered, solvent was removed by rotary evapn., recrystd. (Et2O/petroleum ether); elem. anal.;
References:
Saxena, Arvind K.;Bisaria, Chandra S.;Pande, Lalit M. [Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,1986,vol. 16,p. 667 - 674]