Phosphoric acid, ethenyl diphenyl ester synthesis
2synthesis methods
- Product Name:Phosphoric acid, ethenyl diphenyl ester
- CAS Number:33552-07-7
- Molecular formula:C14H13O4P
- Molecular Weight:276.22
Yield:33552-07-7 70%
Reaction Conditions:
Stage #1: tetrahydrofuranwith n-butyllithium in hexane at 0 - 25; for 18.5 h;
Stage #2: chlorophosphoric acid diphenyl ester at -78 - 20; for 0.75 h;
References:
Kumpulainen, Hanna;Jaervinen, Tomi;Saari, Raimo;Lehtonen, Marko;Vepsaelaeinen, Jouko [Journal of Organic Chemistry,2005,vol. 70,# 22,p. 9056 - 9058]
