PHOSPHOROUS ACID TRIS(4-METHYLPHENYL) ESTER synthesis
- Product Name:PHOSPHOROUS ACID TRIS(4-METHYLPHENYL) ESTER
- CAS Number:620-42-8
- Molecular formula:C21H21O3P
- Molecular Weight:352.36
106-44-5
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$14.00/5g
620-42-8
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$36.10/25G
Yield: 92%
Reaction Conditions:
Stage #1:p-cresol with sodium hydride in tetrahydrofuran at 0 - 20;Inert atmosphere;
Stage #2: with triethylamine;phosphorus trichloride in tetrahydrofuran at 20; for 20 h;Inert atmosphere;
References:
Ho, Chun-Yu;Chan, Chun-Wa;Wo, Siu-Kwan;Zuo, Zhong;Chan, Lai-Ying [Organic and Biomolecular Chemistry,2010,vol. 8,# 15,p. 3480 - 3487] Location in patent:supporting information; experimental part
