Piperazinone, 1,4-dimethyl-3-thioxo- (9CI) synthesis

1synthesis methods

Product Name:Piperazinone, 1,4-dimethyl-3-thioxo- (9CI)
CAS Number:195048-48-7
Molecular formula:C6H10N2OS
Molecular Weight:158.2214

59417-06-0 Synthesis

59417-06-0
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Piperazinone, 1,4-dimethyl-3-thioxo- (9CI)

195048-48-7
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Yield:195048-48-7 59.3%

Reaction Conditions:

with Lawessons reagent in toluene;Reflux;

References:

Pilia, Luca;Artizzu, Flavia;Espa, Davide;Marchio, Luciano;Mercuri, Maria Laura;Serpe, Angela;Deplano, Paola [Dalton Transactions,2010,vol. 39,# 35,p. 8139 - 8142] Location in patent:supporting information; experimental part