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potassium O-heptyl dithiocarbonate synthesis

1synthesis methods
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Yield:2720-78-7 77.15%

Reaction Conditions:

Stage #1: n-heptan1olwith potassium hydroxide for 4 h;Schlenk technique;Inert atmosphere;
Stage #2: carbon disulfideSchlenk technique;Inert atmosphere;

References:

Bakly, Ali A.K.;Collison, David;Ahumada-Lazo, Ruben;Binks, David J.;Smith, Matthew;Raftery, James;Whitehead, George F. S.;O'Brien, Paul;Lewis, David J. [Inorganic Chemistry,2021,vol. 60,# 10,p. 7573 - 7583] Location in patent:supporting information