POTASSIUM OCTYLTRIFLUOROBORATE synthesis
- Product Name:POTASSIUM OCTYLTRIFLUOROBORATE
- CAS Number:329976-79-6
- Molecular formula:C8H17BF3.K
- Molecular Weight:220.125
121-43-7
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$15.00/25ml
17049-49-9
100 suppliers
$75.00/25g
329976-79-6
11 suppliers
$657.30/1G
Yield:329976-79-6 71%
Reaction Conditions:
Stage #1: Trimethyl borate;octylmagnesium bromide in tetrahydrofuran at -78 - 0; for 1.83333 h;
Stage #2: with potassium hydrogen difluoride;water in tetrahydrofuran at 0 - 20; for 1.16667 h;
References:
Reichle, Markus A.;Breit, Bernhard [Angewandte Chemie - International Edition,2012,vol. 51,# 23,p. 5730 - 5734] Location in patent:supporting information; experimental part
28741-08-4
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$6.00/250mg
329976-79-6
11 suppliers
$657.30/1G
1279123-63-5
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121-43-7
346 suppliers
$15.00/25ml
17049-49-9
100 suppliers
$75.00/25g
329976-79-6
11 suppliers
$657.30/1G
111-66-0
145 suppliers
$10.00/10ml
329976-79-6
11 suppliers
$657.30/1G
111-83-1
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$12.00/25g
329976-79-6
11 suppliers
$657.30/1G