Propanamide, N-(4-aminophenyl)-N-methyl- synthesis
- Product Name:Propanamide, N-(4-aminophenyl)-N-methyl-
- CAS Number:112077-95-9
- Molecular formula:C10H14N2O
- Molecular Weight:178.23
90918-78-8
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Yield:-
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol; for 4 h;
Steps:
1.3
Step 3: Synthesis of N-(4-aminophenyl)-N-methylpropionamidePalladium and carbon (10%) was added to the solution of N-methyl-N-(4-nitrophenyl) propionamide (1.17g) in methanol (3OmL). The reaction was stirred under hydrogen for 4 hours. The solution was filtered through celite and used for next step without purification. MS m/z: 179.23 (M+1).
References:
WO2010/129053,2010,A2 Location in patent:Page/Page column 113-114
4850-93-5
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100-01-6
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