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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
684-23-1

Propane, 2-diazo-1,1,1,3,3,3-hexafluoro- synthesis

5synthesis methods
2-Propanone, 1,1,1,3,3,3-hexafluoro-, hydrazone

1588-41-6
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Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-

684-23-1
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Yield:684-23-1 76-79

Reaction Conditions:

with lead(IV) acetate in benzonitrile;addn. of (CF3)2CNNH2 soln. in C6H5CN to suspension of Pb(CH3COO)4 in C6H5CN, mixing at 0°C under N2, warming to 20°C, mixing (1 h);

References:

Gale,D.M. et al. [Journal of the American Chemical Society,1966,vol. 88,p. 3617 - 3623] Middleton, W. J.;Gale, D. M. [Organic Syntheses,1970,vol. 50,p. 6 - 9]

1,1,1,3,3,3-HEXAFLUOROISOPROPYLAMINE

1619-92-7
33 suppliers
$25.00/250mg

Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-

684-23-1
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References
1619-91-6 Synthesis
1,1,1,3,3,3-Hexafluoroprop-2-ylaMine hydrochloride

1619-91-6
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7632-00-0 Synthesis
Sodium nitrite

7632-00-0
887 suppliers
$14.00/25g

Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-

684-23-1
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References
3,3-Bis(trifluoromethyl)-3H-diazirine

3024-50-8
2 suppliers
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Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-

684-23-1
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References
BIS(TRIFLUOROMETHYL)NITROXIDE

2154-71-4
4 suppliers
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2-Propanone, 1,1,1,3,3,3-hexafluoro-, hydrazone

1588-41-6
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359-63-7 Synthesis
N,N-BIS(TRIFLUOROMETHYL)HYDROXYLAMINE

359-63-7
8 suppliers
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Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-

684-23-1
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References