ChemicalBook CAS DataBase List PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]-

PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]- synthesis

4synthesis methods

Product Name:PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]-
CAS Number:22584-31-2
Molecular formula:C5H11N3
Molecular Weight:113.16

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107-13-1 Synthesis

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PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]-

22584-31-2
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Yield:22584-31-2 98.5 %Chromat.

Reaction Conditions:

with porous hyper-cross-linked polymer containing 2.87 mmol/g of ionic liquid embedded in framework synthesized from 4-vinylpyridine and p-xylylene dichloride in neat (no solvent) at 25; for 0.116667 h;Michael Addition;

Steps:

The Procedure for aza-Michael Addition

General procedure: Requisite amounts of amines (20 mmol), alkenes (24 mmol) and catalyst (20 mg) were mixed and reacted for definite time intervals at ambient temperature. The GC analysis was conducted to monitor the reaction process. On completion, the catalyst was recycled by filtration. The recycled catalyst was washed with ethanol and dried at 80°C overnight. Activity of the recycled system was carefully investigated.

References:

Li, Junqiao;Lu, Wei;Li, Weifeng;Liang, Xuezheng [Kinetics and Catalysis,2016,vol. 57,# 6,p. 840 - 846]

107-15-3
9 suppliers
$11.19/25ML

107-13-1 Synthesis

107-13-1
399 suppliers
$19.00/25ML