ChemicalBook CAS DataBase List Propanoic acid, 2-Methyl-2-[(phenylMethyl)thio]-

Propanoic acid, 2-Methyl-2-[(phenylMethyl)thio]- synthesis

7synthesis methods

Product Name:Propanoic acid, 2-Methyl-2-[(phenylMethyl)thio]-
CAS Number:36038-77-4
Molecular formula:C11H14O2S
Molecular Weight:210.29

600-00-0 Synthesis

600-00-0
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$13.00/5g

100-53-8
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$10.00/1g

Propanoic acid, 2-Methyl-2-[(phenylMethyl)thio]-

36038-77-4
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Yield:36038-77-4 80%

Reaction Conditions:

Stage #1: ethyl 2-bromoisobutyrate;phenylmethanethiolwith sodium methylate in ethanol at 90; for 3.5 h;Inert atmosphere;Schlenk technique;
Stage #2: with sodium hydroxide in ethanol;Inert atmosphere;Schlenk technique;

References:

Villar-Acevedo, Gloria;Lugo-Mas, Priscilla;Blakely, Maike N.;Rees, Julian A.;Ganas, Abbie S.;Hanada, Erin M.;Kaminsky, Werner;Kovacs, Julie A. [Journal of the American Chemical Society,2017,vol. 139,# 1,p. 119 - 129] Location in patent:supporting information

Propanoic acid, 2-(2-benzothiazolylthio)-2-methyl-

65937-38-4
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100-39-0
424 suppliers
$10.00/10g

36038-77-4
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Propanoic acid, 2-methyl-2-[(phenylmethyl)thio]-, methyl ester

87122-84-7
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36038-77-4
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Propanoic acid, 2-methyl-2-[(phenylmethyl)thio]-, ethyl ester

62738-24-3
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36038-77-4
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100-39-0
424 suppliers
$10.00/10g

4695-31-2
63 suppliers
$155.00/500mg

36038-77-4
13 suppliers
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