![](/CAS/GIF/109-60-4.gif)
Propyl acetate synthesis
- Product Name:Propyl acetate
- CAS Number:109-60-4
- Molecular formula:C5H10O2
- Molecular Weight:102.13
![1-Propanol](/CAS/GIF/71-23-8.gif)
71-23-8
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50373-55-2
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![Propyl acetate](/CAS/GIF/109-60-4.gif)
109-60-4
559 suppliers
$18.00/25mL
![(R)-(+)-1-Phenylethanol](/CAS/GIF/1517-69-7.gif)
1517-69-7
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$6.00/1g
![Acetic Acid (S)-1-Phenylethyl Ester](/CAS/20200119/GIF/16197-93-6.gif)
16197-93-6
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![Acetic Acid (R)-1-Phenylethyl Ester](/CAS/20180808/GIF/16197-92-5.gif)
16197-92-5
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Yield:99.9 % ee , 69.2 % ee
Reaction Conditions:
with Candida antarctica lipase immobilized on acrylic resine in di-isopropyl ether at 40; for 24 h;Enzymatic reaction;enantioselective reaction;Solvent;
Steps:
2.5 General Procedure for the Alcoholysis of Racemic Acetates (1a-7a) with Candida antarctica- B lipase
General procedure: To 1 mmol of the racemic acetates (1a-7a) dissolved in Scheme 1 Possible pathways for enzymatic deacetylation of acetate 2 mL of organic solvent, 2 mmol of the appropriate alcohol and 12 mg of CAL-B, are added. The suspension was stirred at 40 °C for 24 h. The reaction mixture is filtered on Celite and concentrated in vacuo. The remaining acetate and the producing alcohol were separated by chromatography on silica gel (petroleum ether/ethyl acetate: 80/20) and analyzed by chiral GC. The same procedure was followed for the reactions in the presence of 60 mg of molecular sieves 4 ?.
References:
Zadi, Amna;Merabet-Khelassi, Mounia;Aribi-Zouioueche, Louisa [Catalysis Letters,2015,vol. 145,# 4,art. no. 1470,p. 1054 - 1061]
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591-87-7
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![Propyl acetate](/CAS/GIF/109-60-4.gif)
109-60-4
559 suppliers
$18.00/25mL
![1-Propanol](/CAS/GIF/71-23-8.gif)
71-23-8
748 suppliers
$12.00/100g
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64-19-7
1535 suppliers
$10.00/25ML
![Propyl acetate](/CAS/GIF/109-60-4.gif)
109-60-4
559 suppliers
$18.00/25mL
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64-19-7
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$10.00/25ML
![Propyl acetate](/CAS/GIF/109-60-4.gif)
109-60-4
559 suppliers
$18.00/25mL
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764-47-6
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![Propyl acetate](/CAS/GIF/109-60-4.gif)
109-60-4
559 suppliers
$18.00/25mL