Pseudo protopine synthesis

9synthesis methods

Product Name:Pseudo protopine
CAS Number:24240-05-9
Molecular formula:C20H19NO5
Molecular Weight:353.37

2606-51-1 Synthesis

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24240-05-9
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 83 percent / NaH / tetrahydrofuran; dimethylformamide / Heating
2: 70 percent / phosphoryl chloride / toluene / 5 h / Heating
3: O₂ / 0.17 h / 18 - 20 °C / Irradiation
4: lithium aluminum hydride / tetrahydrofuran / 3 h / Heating
5: 85 percent / MnO₂ / CHCl₃ / 1 h / Ambient temperature

References:

Orito, Kazuhiko;Kudoh, Shigekazu;Yamada, Kinji;Itoh, Mitsuomi [Heterocycles,1980,vol. 14,# 1,p. 11 - 14]

Bis[1,3]benzodioxolo[5,6-c:5',6'-g]azecin-14-ol, 5,6,7,8,14,15-hexahydro-6-methyl-

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24240-05-9
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6H-1,3-Dioxolo[4,5-h][3]benzazepin-6-one, 5,7,8,9-tetrahydro-7-methyl-

74059-70-4
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24240-05-9
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References

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58937-72-7
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24240-05-9
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References

Bis[1,3]benzodioxolo[5,6-c:5',6'-g]azecine-5,14(6H,15H)-dione, 7,8-dihydro-6-methyl-

74059-76-0
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24240-05-9
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References