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1199809-32-9

PSI-938 synthesis

12synthesis methods
Guanosine, 2'-deoxy-6-O-ethyl-2'-fluoro-2'-methyl-, cyclic 3',5'-[1-methylethyl (R)-phosphite], (2'R)-

1294481-83-6
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PSI-938

1199809-32-9
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Yield:1199809-32-9 80.5 g

Reaction Conditions:

with pyridine;water;iodine in tetrahydrofuran at 5 - 10; for 2 h;

References:

Reddy, P. Ganapati;Chun, Byoung-Kwon;Zhang, Hai-Ren;Rachakonda, Suguna;Ross, Bruce S.;Sofia, Michael J. [Journal of Organic Chemistry,2011,vol. 76,# 10,p. 3782 - 3790] Location in patent:experimental part