Pyridine, 2,2',2''-phosphinidynetris[6-methyl- synthesis
- Product Name:Pyridine, 2,2',2''-phosphinidynetris[6-methyl-
- CAS Number:131504-44-4
- Molecular formula:C18H18N3P
- Molecular Weight:307.3294
5315-25-3
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Yield:131504-44-4 62%
Reaction Conditions:
Stage #1: 2-bromo-6-methylpyridinewith n-butyllithium in diethyl ether;hexane at -78; for 3 h;Inert atmosphere;
Stage #2: with phosphorus trichloride in diethyl ether at -78 - 20;Inert atmosphere;
References:
Bond, Andrew D.;García-Rodríguez, Raúl;Hanf, Schirin;Hey-Hawkins, Evamarie;Wright, Dominic S. [Dalton Transactions,2016,vol. 45,# 1,p. 276 - 283]