PYRIDINE-2-CARBONYL AZIDE synthesis
- Product Name:PYRIDINE-2-CARBONYL AZIDE
- CAS Number:4013-71-2
- Molecular formula:C6H4N4O
- Molecular Weight:148.12
98-98-6
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Yield:4013-71-2 85%
Reaction Conditions:
Stage #1: 2-Picolinic acidwith (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate;N-ethyl-N,N-diisopropylamine in tetrahydrofuran at 0; for 0.333333 h;
Stage #2: with sodium azide in tetrahydrofuran;dimethyl sulfoxide at 0; for 0.25 h;
References:
Vasantha;Sureshbabu, Vommina V. [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2010,vol. 49,# 6,p. 812 - 817] Location in patent:experimental part
40086-66-6
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4013-71-2
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39901-94-5
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$21.00/1g
4013-71-2
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144223-29-0
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$106.00/1g
4013-71-2
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