ChemicalBook CAS DataBase List Pyridine, 3-(1-Methylethenyl)-

Pyridine, 3-(1-Methylethenyl)- synthesis

11synthesis methods

Product Name:Pyridine, 3-(1-Methylethenyl)-
CAS Number:15825-89-5
Molecular formula:C8H9N
Molecular Weight:119.16

626-55-1 Synthesis

626-55-1
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108-22-5 Synthesis

108-22-5
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$20.00/25mL

15825-89-5
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Yield:15825-89-5 96%

Reaction Conditions:

Stage #1: 3-Bromopyridinewith magnesium;lithium chloride in tetrahydrofuran at 0 - 20; for 2 h;Schlenk technique;Inert atmosphere;
Stage #2: Isopropenyl acetatewith iron(III) chloride in tetrahydrofuran at 0; for 3 h;Schlenk technique;Inert atmosphere;

References:

G?rtner, Dominik;Stein, André Luiz;Grupe, Sabine;Arp, Johannes;Von Wangelin, Axel Jacobi [Angewandte Chemie - International Edition,2015,vol. 54,# 36,p. 10545 - 10549][Angew. Chem.,2015,vol. 127,# 36,p. 10691 - 10695,5] Location in patent:supporting information

626-60-8 Synthesis