Pyridine, 3-hydrazino-2-methoxy- (9CI) synthesis
- Product Name:Pyridine, 3-hydrazino-2-methoxy- (9CI)
- CAS Number:160590-38-5
- Molecular formula:C6H9N3O
- Molecular Weight:139.16
20265-38-7
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Yield:160590-38-5 88%
Reaction Conditions:
Stage #1: 3-amino-2-methoxypyridinewith hydrogenchloride;sodium nitrite in water at 0; for 0.5 h;
Stage #2: with hydrogenchloride;tin(II) chloride dihdyrate in water at 0; for 1.5 h;
Stage #3: with potassium hydroxide in water;
References:
Jeanty, Matthieu;Blu, Jerome;Suzenet, Franck;Guillaumet, Gerald [Organic Letters,2009,vol. 11,# 22,p. 5142 - 5145] Location in patent:supporting information; experimental part
13472-59-8
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