Pyridine, 4,4'-(2,5-difluoro-1,4-phenylene)bis- synthesis
1synthesis methods
- Product Name:Pyridine, 4,4'-(2,5-difluoro-1,4-phenylene)bis-
- CAS Number:1429342-59-5
- Molecular formula:C16H10F2N2
- Molecular Weight:268.26
Yield:1429342-59-5 1.5 mmol
Reaction Conditions:
with potassium phosphate;tris-(dibenzylideneacetone)dipalladium(0);tricyclohexylphosphine in 1,4-dioxane;water at 100; for 18 h;Inert atmosphere;Schlenk technique;Suzuki Coupling;
References:
Culp, Jeffrey T.;Madden, Catherine;Kauffman, Kristi;Shi, Fan;Matranga, Christopher [Inorganic Chemistry,2013,vol. 52,# 8,p. 4205 - 4216] Location in patent:supporting information