quiditene synthesis
- Product Name:quiditene
- CAS Number:57734-76-6
- Molecular formula:C16H20ClNOS2
- Molecular Weight:341.9191
188290-36-0
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6238-33-1
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591-51-5
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57734-76-6
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Yield:57734-76-6 67.4%
Reaction Conditions:
Stage #1: bromobenzenewith lithium in diethyl ether; for 1 h;Heating;Metallation;
Stage #2: thiophene;phenyllithium at 25; for 0.75 h;Addition;
Stage #3: 3-quinuclidinecarboxylic acid ethyl ester in diethyl ether at -10 - -5; for 0.5 h;Condensation;
References:
Koikov, L. N.;Polikarpov, M. V.;Alekseeva, N. V.;Obydenova, T. A.;Turchin, K. F.;Filipenko, T. Ya. [Pharmaceutical Chemistry Journal,1998,vol. 32,# 10,p. 546 - 549][Khimiko-Farmatsevticheskii Zhurnal,1998,vol. 32,# 10,p. 34 - 37]
188290-36-0
1 suppliers
inquiry
108-86-1
498 suppliers
$10.00/5g
6238-33-1
25 suppliers
inquiry
57734-76-6
12 suppliers
$199.00/500mg