![](/CAS/GIF/23357-46-2.gif)
(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine synthesis
- Product Name:(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine
- CAS Number:23357-46-2
- Molecular formula:C10H13N
- Molecular Weight:147.22
![1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/2217-40-5.gif)
2217-40-5
185 suppliers
$10.00/1g
![Glyoxylic acid](/CAS/GIF/298-12-4.gif)
298-12-4
438 suppliers
$5.00/25g
![(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/23357-46-2.gif)
23357-46-2
152 suppliers
$7.00/1g
![1-Tetralone](/CAS/GIF/529-34-0.gif)
529-34-0
478 suppliers
$6.00/10g
Yield:> 99 % ee
Reaction Conditions:
with pyridoxal 5'-phosphate;recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. buffer at 37; pH=7.4; for 12 h;Resolution of racemate;Enzymatic reaction;enantioselective reaction;
Steps:
2.9. Kinetic resolution of racemic amines
General procedure: Racemic amine (10 mM, Table 4) was mixed with glyoxylate (10 mM) in 1 ml of phosphate buffer (100 mM, pH 7.4) containing PLP (20 μM). The reaction was started by adding 0.8 mg/ml of HBV-ω-TA, and the mixture was incubated at 37 °C for 12 h. The amount and ee value of the residual amino donor were determined according to Section 2.10.
References:
Jiang, Jinju;Chen, Xi;Feng, Jinhui;Wu, Qiaqing;Zhu, Dunming [Journal of Molecular Catalysis B: Enzymatic,2014,vol. 100,p. 32 - 39]
![1-Tetralone](/CAS/GIF/529-34-0.gif)
529-34-0
478 suppliers
$6.00/10g
![(S)-1,2,3,4-Tetrahydro-1-naphthalenamine](/CAS/GIF/23357-52-0.gif)
23357-52-0
154 suppliers
$8.00/1g
![(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/23357-46-2.gif)
23357-46-2
152 suppliers
$7.00/1g
![1,2,3,4-Tetrahydronaphthalene](/CAS/GIF/119-64-2.gif)
119-64-2
329 suppliers
$9.00/25g
![(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/23357-46-2.gif)
23357-46-2
152 suppliers
$7.00/1g
![1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/2217-40-5.gif)
2217-40-5
185 suppliers
$10.00/1g
![(S)-1,2,3,4-Tetrahydro-1-naphthalenamine](/CAS/GIF/23357-52-0.gif)
23357-52-0
154 suppliers
$8.00/1g
![(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/23357-46-2.gif)
23357-46-2
152 suppliers
$7.00/1g
![Naphthalene, 1-azido-1,2,3,4-tetrahydro-, (1R)-](/CAS/20211123/GIF/1055321-32-8.gif)
1055321-32-8
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![(R)-(-)-1,2,3,4-Tetrahydro-1-naphthylamine](/CAS/GIF/23357-46-2.gif)
23357-46-2
152 suppliers
$7.00/1g