ChemicalBook CAS DataBase List (R)-N-Fmoc-2-(4'-pentenyl)glycine

(R)-N-Fmoc-2-(4'-pentenyl)glycine synthesis

2synthesis methods

Product Name:(R)-N-Fmoc-2-(4'-pentenyl)glycine
CAS Number:1093645-21-6
Molecular formula:C22H23NO4
Molecular Weight:365.42

1119-51-3 Synthesis

1119-51-3
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1093645-21-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: potassium hydroxide; C₃₇H₃₉N₂O⁽¹⁺⁾ / dichloromethane / 0.17 h / -50 °C / Inert atmosphere
1.2: -50 - 20 °C
2.1: citric acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
3.1: sodium carbonate / 1,4-dioxane; water / 0.17 h / 0 °C
3.2: 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

References:

McWhinnie, Fergus S.;Sepp, Kristel;Wilson, Charlotte;Kunath, Tilo;Hupp, Ted R.;Baker, Terry S.;Houston, Douglas R.;Hulme, Alison N. [Chemistry - A European Journal,2018,vol. 24,# 9,p. 2094 - 2097]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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1093645-21-6
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$65.00/10mg

References