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ChemicalBook CAS DataBase List RebaMipide 3-Chloro IMpurity
90098-05-8

RebaMipide 3-Chloro IMpurity synthesis

3synthesis methods
4876-10-2 Synthesis
4-Bromomethyl-1,2-dihydroquinoline-2-one

4876-10-2
310 suppliers
$5.00/5g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 69 percent / sodium / ethanol / 2 h
2: 89 percent / 20 percent hydrochloric acid / 9 h / Heating
3: 54 percent / K2CO3 / acetone; H2O

References:

Uchida;Tabusa;Komatsu;Morita;Kanbe;Nakagawa [Chemical and Pharmaceutical Bulletin,1985,vol. 33,# 9,p. 3775 - 3786]

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