ChemicalBook CAS DataBase List rhodiocyanoside A

rhodiocyanoside A synthesis

5synthesis methods

Product Name:rhodiocyanoside A
CAS Number:168433-86-1
Molecular formula:C11H17NO6
Molecular Weight:259.26

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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 25 percent / β-glucosidase, phosphate buffer, pH 5 / 24 h / 30 °C
2: 98 percent / pyridine, 4-dimethylaminopyridine / 0.25 h / Ambient temperature
3: 1.) O₃, 2.) Me₂S / 1.) CH₂Cl₂, -78 deg C, 2 h, 2.) CH₂Cl₂, RT, 30 min
4: 1.) NaH / 1.) n-hexane, THF, 0 deg C, 15 min, 2.) n-hexane, THF, 0 deg C, 30 min
5: 77 percent / K₂CO₃ / methanol / 0.5 h / Ambient temperature

References:

Akita, Hiroyuki;Kurashima, Katsumi;Nakamura, Takuya;Kato, Keisuke [Tetrahedron Asymmetry,1999,vol. 10,# 12,p. 2429 - 2439]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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β-D-Glucopyranoside, 3-methyl-2-buten-1-yl

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References