(S)-2-Chlorophenylglycinol synthesis
- Product Name:(S)-2-Chlorophenylglycinol
- CAS Number:213990-63-7
- Molecular formula:C8H10ClNO
- Molecular Weight:171.62
141315-50-6
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$10.00/5g
213990-63-7
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$155.00/250MG
Yield:213990-63-7 92%
Reaction Conditions:
Stage #1: (S)-2-chlorophenylglycinewith sodium tetrahydroborate in tetrahydrofuran; for 0.166667 h;Sealed tube;Inert atmosphere;Cooling with ice;
Stage #2: with iodine in tetrahydrofuran; for 16 h;Sealed tube;Inert atmosphere;Reflux;
References:
Liu, En-Chih;Topczewski, Joseph J. [Journal of the American Chemical Society,2019,vol. 141,# 13,p. 5135 - 5138] Location in patent:supporting information