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ChemicalBook CAS DataBase List (S)-3-AMINO-3-(3-NITRO-PHENYL)-PROPIONIC ACID

(S)-3-AMINO-3-(3-NITRO-PHENYL)-PROPIONIC ACID synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 70 °C / Large scale
2.1: zinc / tetrahydrofuran / 1 h / 40 - 50 °C / Inert atmosphere; Darkness
2.2: 20 °C
3.1: lithium hydroxide; water / tetrahydrofuran / 1 h / 5 - 20 °C
4.1: hydrogenchloride / ethyl acetate / 2 h / 5 - 20 °C

References:

Shenzhen Yinnuosheng Biological Technology Co., Ltd.;Lin Wenquan;Qiu Xuehui;Wu Jiangqin CN108976141, 2018, A

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