S-(4-FLUOROPHENYL)MERCAPTURIC ACID synthesis
3synthesis methods
- Product Name:S-(4-FLUOROPHENYL)MERCAPTURIC ACID
- CAS Number:331-93-1
- Molecular formula:C11H12FNO3S
- Molecular Weight:257.28
Yield:331-93-1 99%
Reaction Conditions:
Stage #1: N-acetylcystein;4-fluoro-1-iodobenzenewith C53H46NO4PPdS in tetrahydrofuran at 20; for 0.0166667 h;Schlenk technique;
Stage #2: with triethylamine in tetrahydrofuran at 20; for 0.0833333 h;Schlenk technique;Inert atmosphere;chemoselective reaction;
References:
Al-Shuaeeb, Riyadh Ahmed Atto;Kolodych, Sergii;Koniev, Oleksandr;Delacroix, Sébastien;Erb, Stéphane;Nicola?, Stéphanie;Cintrat, Jean-Christophe;Brion, Jean-Daniel;Cianférani, Sarah;Alami, Mouad;Wagner, Alain;Messaoudi, Samir [Chemistry - A European Journal,2016,vol. 22,# 32,p. 11365 - 11370] Location in patent:supporting information
