(S)-(-)-4-PHENYL-1,3-DIOXANE synthesis
- Product Name:(S)-(-)-4-PHENYL-1,3-DIOXANE
- CAS Number:107796-30-5
- Molecular formula:C10H12O2
- Molecular Weight:164.2
110-88-3
226 suppliers
$13.00/100g
100-42-5
617 suppliers
$20.00/25mL
107796-30-5
7 suppliers
inquiry
107796-29-2
6 suppliers
inquiry
Yield:85 % ee
Reaction Conditions:
with 1,1,1-trifluoro-N-((11bS)-4-(((11bS)-4-oxido-2,6-bis(4-(trifluoromethyl)phenyl)dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)imino)-2,6-bis(4-(trifluoromethyl)phenyl)-4λ5-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)methanesulfonamide in cyclohexane at 25; for 48 h;Inert atmosphere;Schlenk technique;Overall yield = 11 percentSpectr.; enantioselective reaction;Prins-Kriewitz Hydroxyinethylation;
References:
Diáz-Oviedo, C. David;Maji, Rajat;List, Benjamin [Journal of the American Chemical Society,2021,vol. 143,# 49,p. 20598 - 20604] Location in patent:supporting information
100-42-5
617 suppliers
$20.00/25mL
50-00-0
846 suppliers
$10.00/25g
107796-30-5
7 suppliers
inquiry
107796-29-2
6 suppliers
inquiry