ChemicalBook CAS DataBase List (S)-Methyl (1-aMinopropan-2-yl)carbaMate

(S)-Methyl (1-aMinopropan-2-yl)carbaMate synthesis

2synthesis methods

Product Name:(S)-Methyl (1-aMinopropan-2-yl)carbaMate
CAS Number:1229025-89-1
Molecular formula:C5H12N2O2
Molecular Weight:132.16

14568-46-8 Synthesis

Carbamic acid, N-[(1S)-2-hydroxy-1-methylethyl]-, methyl ester

14568-46-8
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(S)-Methyl (1-aMinopropan-2-yl)carbaMate

1229025-89-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 3 h / 20 °C
1.2: 2 h / 80 °C
2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h / 20 °C / 760.05 Torr

References:

IRM LLC;NOVARTIS AG;HUANG, Shenlin;JIN, Xianming;LIU, Zuosheng;POON, Daniel;TELLEW, John;WAN, Yongqin;WANG, Xing;XIE, Yongping WO2011/25927, 2011, A1

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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1229025-89-1
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References