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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List savinin
493-95-8

savinin synthesis

6synthesis methods
2373-80-0 Synthesis
3,4-(Methylenedioxy)cinnamic acid

2373-80-0
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$12.00/10g

savinin

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-

Yield:-

Steps:

Multi-step reaction with 8 steps
1: 100 percent / H2 / Pd/C / dimethylformamide / 24 h / 760 Torr
2: 1.) pivaloyl chloride, 2.) BuLi
3: 1.) NaHMDS / 1.) THF, -73 deg C, 1 h, 2.) THF, 2 h
4: 30percent aq.H2O2, LiOH*H2O / tetrahydrofuran / 3 h / Ambient temperature
5: BH3*THF / 4 h / Ambient temperature
6: TFA / CH2Cl2 / 3 h / Ambient temperature
7: 1.) NaHMDS, 3.) Et3N, DMAP
8: DBU / toluene / 1.5 h / 80 °C

References:

Charlton, James L.;Chee, Gaik-Lean [Canadian Journal of Chemistry,1997,vol. 75,# 8,p. 1076 - 1083]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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savinin

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References
3-(3,4-METHYLENEDIOXYPHENYL)PROPIONIC ACID

2815-95-4
110 suppliers
$22.00/1g

savinin

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References
2(3H)-Furanone, 4-(1,3-benzodioxol-5-ylmethyl)dihydro-, (4R)-

17187-77-8
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savinin

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References
2-Oxazolidinone, 3-[3-(1,3-benzodioxol-5-yl)-1-oxopropyl]-4-(1-methylethyl)-, (4S)-

161745-67-1
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savinin

493-95-8
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References

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