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ChemicalBook CAS DataBase List savinin

savinin synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 8 steps
1: 100 percent / H2 / Pd/C / dimethylformamide / 24 h / 760 Torr
2: 1.) pivaloyl chloride, 2.) BuLi
3: 1.) NaHMDS / 1.) THF, -73 deg C, 1 h, 2.) THF, 2 h
4: 30percent aq.H2O2, LiOH*H2O / tetrahydrofuran / 3 h / Ambient temperature
5: BH3*THF / 4 h / Ambient temperature
6: TFA / CH2Cl2 / 3 h / Ambient temperature
7: 1.) NaHMDS, 3.) Et3N, DMAP
8: DBU / toluene / 1.5 h / 80 °C

References:

Charlton, James L.;Chee, Gaik-Lean [Canadian Journal of Chemistry,1997,vol. 75,# 8,p. 1076 - 1083]

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