ChemicalBook CAS DataBase List SELACHYL ALCOHOL

SELACHYL ALCOHOL synthesis

5synthesis methods

Product Name:SELACHYL ALCOHOL
CAS Number:593-31-7
Molecular formula:C21H42O3
Molecular Weight:342.56

1,3-Dioxolane, 2,2-dimethyl-4-[[(9Z)-9-octadecen-1-yloxy]methyl]-

22610-35-1
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593-31-7
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Yield:593-31-7 28.1%

Reaction Conditions:

with boric acid

Steps:

1
Example 1-Preparation of GEO GLYCERYL-1-MONOOLEATE ether (GEO, also abbreviated to GME) can be obtained commercially from NIKKOL(at) Japan in 95% purity. GEO of greater purity was synthesised by the reaction of 1,2-isopropylidene glycerol potassium salt and oleyl p-toluene sulphonate as indicated in the reaction scheme below. The progress of the reaction was followed by TLC. 0 -as// 0/0 0 X 0 'pK zu 0 °A0 e 0 Yield 60. 9% H3BO3 HO HO HO Yield 28. 1% Purity 99. 6%

References:

CAMURUS AB;GODDARD, Chris WO2005/27976, 2005, A2 Location in patent:Page/Page column 24

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